摘要:金针菇多糖(Flammulina velutipes polysaccharides)对人体有多种保健功效,具有重要的开发价值。金针菇下脚料成本低廉,可提取金针菇多糖及活性炭。本实验主要研究金针菇下脚料利用热水浸提法提取金针菇多糖以及制备活性炭的工艺研究。通过单因子及SAS优化设计,获得了多糖提取最优条件:浸提温度100℃、pH为5.9、料液比为1:15、浸提时间3.47 h,多糖提取率达到42.65mg/g,较未优化提高了3.8倍;通过单因子优化,获得了微波炭化制备活性炭的最适条件:50%的磷酸活化8 h、中火、炭化5 min,制备的活性炭对亚甲基蓝的吸附能力达到81.22mg/g,吸附率达到95.33%。本论文研究为金针菇下脚料的资源化开发提供理论依据及技术支撑。
关键词:金针菇下脚料,金针菇多糖,活性炭,提取
Abstract: Flammulina velutipes polysaccharides have many health benefits for human being, making it a magnificent value for development. Flammulina velutipe offcuts are low-cost and can be extracted with polysaccharide and activated carbon. This experiment in primary studies extracting polysaccharide and a process of preparation of activated carbon from flammulina velutipe cutoffs by using hot water. Through single-factor and SAS optimization design, an optimal condition of having polysaccharide is obtained: an extraction temperature of 100 ℃, a pH of 5.9, a solid-liquid ratio of 1:15 and a leaching period of 3.47 h. The polysaccharide extraction yield acquired is 42.65 mg/g which has 3.8 times increase in comparison to the last optimization; With single factor optimization, the optimum condition of using microwave carbonization to prepare activated carbon is achieved: 50% phosphoric in activation for 8 hours, medium baking and carbonization for 5 min. the achieved activated carbon has a capacity of adsorbing methylene in 81.22 mg/g, with an adsorption rate of 95.33%. This study provides theoretical basis and technical supports for Flammulina velutipe cutoff resource development.
Keywords: Flammulina velutipe cutoffs, Flammulina velutipe polysaccharide, activated carbon, extraction
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